WO2025223878 - METHOD FOR PREPARING AN EXTRUDED CATALYST BASED ON CATALYST FINES WITHOUT FINAL CALCINATION

National phase entry is expected:
Publication Number WO/2025/223878
Publication Date 30.10.2025
International Application No. PCT/EP2025/060016
International Filing Date 11.04.2025
Title **
[English] METHOD FOR PREPARING AN EXTRUDED CATALYST BASED ON CATALYST FINES WITHOUT FINAL CALCINATION
[French] PROCEDE DE PREPARATION D'UN CATALYSEUR EXTRUDÉ À BASE DE FINES DE CATALYSEUR SANS CALCINATION FINALE
Applicants **
IFP ENERGIES NOUVELLES
Inventors
DELPOUX, Olivier
DEVERS, Elodie
Priority Data
FR2404394   26.04.2024   FR
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Quotation for National Phase entry

Country StagesTotal
China Filing, Examination, Granting2110
EPO Filing, Examination, Granting8406
Japan Filing, Examination, Granting2154
South Korea Filing, Examination, Granting2066
USA Filing, Examination, Granting4740
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Abstract[English] A method for preparing a catalyst from catalyst fines comprising a group VIB metal, a group VIII metal, and an oxide support, said fines having a D90 size of less than or equal to 500 micrometers, the method comprising the following steps: a) mixing said fines and an extrusion aid, and optionally an inorganic oxide binder; b) kneading the mixture obtained in step a) by adding an aqueous solution containing a carboxylic acid; c) optionally adding a neutralizing agent chosen from an inorganic base and an organic base to said mixture obtained in step b); d) shaping the mixture obtained in step b) or c) by extrusion in order to obtain a solid; e) drying the solid obtained in step d) at a temperature below 200°C, without subsequently calcining it.[French] Procédé de préparation d'un catalyseur à partir de fines de catalyseur comprenant un métal du groupe VIB, un métal du groupe VIII, et un support d'oxyde, lesdites fines ayant une taille D90 inférieure ou égale à 500 micromètres, le procédé comprenant les étapes suivantes : a) on mélange lesdites fines et un agent d'aide à l'extrusion, et optionnellement un liant d'oxyde inorganique, b) on effectue un malaxage du mélange obtenu à l'étape a) en ajoutant une solution aqueuse contenant un acide carboxylique, c) on ajoute optionnellement audit mélange obtenu à l'étape b) un agent de neutralisation choisi parmi une base inorganique et une base organique, d) on effectue une mise en forme par extrusion du mélange obtenu à l'étape b) ou c) pour obtenir un solide, e) on sèche le solide obtenu à l'étape d) à une température inférieure à 200°C, sans le calciner ultérieurement.