WO2023006604 - IMPROVEMENTS RELATING TO THE COLD-ALKALI PROCESS FOR THE PRODUCTION OF REGENERATED CELLULOSIC FIBERS

National phase entry:
Publication Number WO/2023/006604
Publication Date 02.02.2023
International Application No. PCT/EP2022/070612
International Filing Date 22.07.2022
Title **
[English] IMPROVEMENTS RELATING TO THE COLD-ALKALI PROCESS FOR THE PRODUCTION OF REGENERATED CELLULOSIC FIBERS
[French] AMÉLIORATIONS SE RAPPORTANT À LA TRANSFORMATION BASIQUE À FROID POUR LA PRODUCTION DE FIBRES CELLULOSIQUES RÉGÉNÉRÉES
Applicants **
LENZING AKTIENGESELLSCHAFT
Inventors
DOBSON, Peter
REDLINGER, Sigrid
Priority Data
21187686.7   26.07.2021   EP
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Quotation for National Phase entry

Country StagesTotal
China Filing, Examination, Granting2024
EPO Filing, Examination, Granting8126
Japan Filing, Examination, Granting2155
South Korea Filing, Examination, Granting2071
USA Filing, Examination, Granting4740
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Total: 19,116

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Abstract[English] The present disclosure relates to a method and processing facility for producing regenerated cellulosic fibers. The method comprises extruding a spinning solution into a coagulation bath which contains a salt and preferably an alkali to produce the fibers. The spinning solution comprising cellulose dissolved in an aqueous solvent comprising NaOH and ZnO. The coagulation bath has a pH-value of at least seven. The method further comprises a continuous process of applying to the fibers in a never-dried state a crosslinking agent with two or more reactive groups and heating the fibers to a curing temperature while maintaining the never-dried condition to produce a reaction between the crosslinking agent and the cellulose of the fiber.[French] La présente invention concerne un procédé et une installation de transformation permettant de produire des fibres cellulosiques régénérées. Le procédé consiste à extruder une solution de filage dans un bain de coagulation qui contient un sel et de préférence une base pour produire les fibres. La solution de filage comprend de la cellulose dissoute dans un solvant aqueux contenant du NaOH et du ZnO. Le bain de coagulation a une valeur de pH supérieure ou égale à sept. Le procédé comprend en outre un processus continu d'application aux fibres, dans un état jamais sec, d'un agent de réticulation comportant deux groupes réactifs ou plus, et de chauffage des fibres à une température de durcissement tout en maintenant l'état jamais sec pour produire une réaction entre l'agent de réticulation et la cellulose de la fibre.