WO2023154166 - SCALABLE METHOD FOR PREPARING CRYSTALLINE BOROSULFATE MATERIALS

National phase entry is expected:
Publication Number WO/2023/154166
Publication Date 17.08.2023
International Application No. PCT/US2023/010736
International Filing Date 13.01.2023
Title **
[English] SCALABLE METHOD FOR PREPARING CRYSTALLINE BOROSULFATE MATERIALS
[French] MÉTHODE ÉVOLUTIVE DE PRÉPARATION DE MATÉRIAUX DE BOROSULFATE CRISTALLIN
Applicants **
THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY
Inventors
CHALOUX, Brian
RIDENOUR, James
EPSHTEYN, Albert
Priority Data
63/307,839   08.02.2022   US
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Quotation for National Phase entry

Country StagesTotal
China Filing, Examination, Granting1957
EPO Filing, Examination, Granting11653
Japan Filing, Examination, Granting1895
South Korea Filing, Examination, Granting1299
USA Filing, Examination, Granting4740
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Total: 21,544

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Abstract[English] present in solution in concentrated sulfuric acid at 5% to 15% by weight is reacted with a cation source at 100–250 °C under dynamic vacuum while in connection with a receiving vessel comprising a desiccant and separate from the reaction vessel, thereby causing formation of a borosulfate material in the reaction vessel while eliminated water is collected in the receiving vessel.[French] présent en solution dans de l'acide sulfurique concentré à 5 % à 15 % en poids est mis à réagir avec une source de cations à 100 à 250°C sous vide dynamique tout en étant en liaison avec un récipient de réception comprenant un déshydratant et séparé du récipient de réaction, provoquant ainsi la formation d'un matériau de borosulfate dans le récipient de réaction tandis que l'eau éliminée est collectée dans le récipient de réception.

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